Table 2 Parameter values for GC/MS

Carrier gas

Helium

Helium cylinders

Column:

capillary column (19,091 F) - General

Size 5 mm

Flow = 0.5 ml/min

Detector:

Mass

Oven:

Gradient

Initial temperature = 65 °C

Rate = 5 °C

Final temperature = 90 °C

Run time = 7.5 min

Inlet:

Temperature = 90 °C

Total flow = 79.5 ml/min

Septum Purge Flow = 3 ml/min

Gas Saver = on

Injector

split less

90 °C